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Triphenylmethyl1 benzyl-type protecting groups1 Amino protecting group1 Organic synthesis containing amines1 benzyloxycarbonyl1 Peptide Chemistry6 condensing reagent2 protecting group7 carboxylic acid30 Tert butyl ester1 Tert butyl protection1 tert-butyl1 Amide bond construction8 TCFH–NMI1 carboxylic acid activation5 ATD-DMAP1 Analytical Instrument1 Comparability Study1 Multi-Attribute Method1 Higher-Order Structure1 Intact Mass Spectrometry1 Glycopeptide Analysis1 Released Glycan Analysis1 Critical Quality Attributes1 Quality Attributes1 Glycoprotein3 Metabolic Disease3 Ceramide2 Insulin Resistance4 O-GlcNAc1 Energy Homeostasis1 Organelle Crosstalk1 Mitochondria16 Redox Metabolism1 Electron Transfer1 New Coupling Reagents1 Inflammation Resolution1 Lipid Droplets2 Sphingolipids3 Leukotrienes1 Prostaglandins1 Immune Regulation4 Inflammatory Response4 Connecting reaction1 sulfur(VI) fluoride exchange1 Receptor Clustering1 Glycocalyx2 Glycolipids1 O-Glycosylation7 N-Glycosylation1